in toluene under protective gas; 8.8 mmol of the Li salt in toluene added to 4 mmol of the Pt complex in toluene at -20°C; mixt. warmed to 20°C and stirred for 2 d; filtration; filtrate evapd. in vac.; fractionated crystn.;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 560, p. 65 - 79
→
反应条件
in toluene mixing of the Mo compd. with the free phosphine (molar ratio 2.0:1) in toluene;; equilibrium;;
参考文献
Polyhedron, , vol. 11, p. 2301 - 2312
→
反应条件
in dichloromethane the Mo compd. was mixed with the free phosphine (molar ratio 1:1) in CH2Cl2 and allowed to react. for 5 days at room temp.;;
参考文献
Poli, Rinaldo; Owens, Beth E.; Krueger, Steven T.; Rheingold, Arnold L.
Polyhedron, 1992 , vol. 11, p. 2301 - 2312
