3-(4-溴苯基)丙酰氯化合成路线 （共 8 条）
反应条件
1: 91 percent / AlCl3 / CS2 2: 89 percent / NaBH4 / ethanol / 25 °C 3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
aluminium trichloride in carbon disulfide
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 91 percent / AlCl3 / CS2
2: 89 percent / NaBH4 / ethanol / 25 °C
3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
4: 93 percent / NiCl2<dppp>2 / diethyl ether / Heating
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: aluminum trichloride / CH2Cl2
2: sodium borohydride / methanol
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 91 percent / AlCl3 / CS2
2: 89 percent / NaBH4 / ethanol / 25 °C
3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
4: 96 percent / NiCl2<dppp>2 / diethyl ether / Heating
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 91 percent / AlCl3 / CS2
2: 89 percent / NaBH4 / ethanol / 25 °C
3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
4: 93 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 91 percent / AlCl3 / CS2
2: 89 percent / NaBH4 / ethanol / 25 °C
3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
4: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 91 percent / AlCl3 / CS2
2: 89 percent / NaBH4 / ethanol / 25 °C
3: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
4: 96 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
