1-羟基-8-甲氧基-9,10-蒽醌合成路线 （共 30 条）
反应条件
1: acetic acid; aqueous HBr 2: sodium acetate View Scheme
参考文献
Naylor; Gardner
Journal of the American Chemical Society, 1931 , vol. 53, p. 4114,4116
反应条件
sodium hydroxide; sodium dithionite 1.) MeOH, water, 70 deg C, 15 min, 2.) MeOH, water, 90 deg C, overnight; Yield given. Multistep reaction;
参考文献
Zembower; Kam; Powers; Zalkow
Journal of Medicinal Chemistry, 1992 , vol. 35, # 9 p. 1597 - 1605
反应条件
sodium hydroxide; sodium dithionite 1.) MeOH, water, 70 deg C, 15 min, 2.) MeOH, water, 90 deg C, overnight; Yield given. Multistep reaction;
参考文献
Zembower; Kam; Powers; Zalkow
Journal of Medicinal Chemistry, 1992 , vol. 35, # 9 p. 1597 - 1605
反应条件
hydrogen bromide; acetic acid
参考文献
Naylor; Gardner
Journal of the American Chemical Society, 1931 , vol. 53, p. 4114,4116
反应条件
hydrogenchloride; tin(ll) chloride in acetic acid Ambient temperature;
参考文献
Prinz, Helge; Wiegrebe, Wolfgang; Mueller, Klaus
Journal of Organic Chemistry, 1996 , vol. 61, # 8 p. 2853 - 2856
反应条件
hydrogen bromide in acetic acid
16 h; Ambient temperature;
参考文献
Zembower; Kam; Powers; Zalkow
Journal of Medicinal Chemistry, 1992 , vol. 35, # 9 p. 1597 - 1605
反应条件
sodium carbonate in various solvent(s)
2 h; Heating;
参考文献
Sereda, Grigoriy A.; Akhvlediani, David G.
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9125 - 9126
反应条件
potassium carbonate in acetone
T=55°C; 24 h; Inert atmosphere;
参考文献
Wei, Li; Hu, Hong-Wen; Lu, Guo-Yuan; Shao, Ying; Zhou, Mi
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 42 p. 8484 - 8492,9
反应条件
sodium hydroxide in ethanol
5 h;
参考文献
Krohn; Muller; Priyono; et al.
1984 , vol. 1984, # 2 p. 306 - 318
反应条件
1: K2CO3 / acetone / 24 h
2: 85 percent / BeCl2 / toluene / 6 h
View Scheme
参考文献
Sharghi, Hashem; Tamaddon, Fatemeh
Tetrahedron, 1996 , vol. 52, # 43 p. 13623 - 13640
