反应条件
1: N,N-(dimethylamino)-methylphenylsulfoxonium tetrafluoroborate With sodium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 0.75 h; Inert atmosphere;
2: (formyl-2H)benzaldehyde in tetrahydrofuran
T=-78°C; 1.5 h; Inert atmosphere;
3: isobutyl phenyl ketene in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere; diastereoselective reaction;
参考文献
Mondal, Mukulesh; Ho, Han-Jen; Peraino, Nicholas J.; Gary, Melanie A.; Wheeler, Kraig A.; Kerrigan, Nessan J.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4587 - 4593
