dihydrogen peroxide; titanium(IV) isopropylate; L-(+)-tartaric acid; silica gel in methanol; water T=25°C; 24 h; Title compound not separated from byproducts;
dihydrogen peroxide; [(η5-C5Me5)Mo(CO)3Cl] in acetonitrile T=-20 - 20°C; 4 h;
参考文献
Gamelas, Carla A.; Lourenco, Tiago; da Costa, Andre Pontes; Simplicio, Ana L.; Royo, Beatriz; Romao, Carlos C.
Tetrahedron Letters, 2008 , vol. 49, # 32 p. 4708 - 4712
(S)-(-)-2-(N-3,5-diiodosalicylidene)amino-3,3-dimethyl-1-butanol; dihydrogen peroxide; p-methoxybenzoic acid Li-salt; Fe(acac)3 in dichloromethane T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 11, # 4 p. 1086 - 1092