4,5-二苯基-1H-1,2,3-三唑合成路线 （共 21 条）
反应条件
tris(4-methylphenyl)bismuth diazide in benzene
3 h; Ambient temperatureIrradiation;
参考文献
Suzuki, Hitomi; Nakaya, Chie; Matano, Yoshihiro
Tetrahedron Letters, 1993 , vol. 34, # 6 p. 1055 - 1056
反应条件
potassium tert-butylate in tetrahydrofuran
T=-78 - 0°C;
参考文献
Yap, Amy H.; Weinreb, Steven M.
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3035 - 3038
反应条件
triethylamine in methanol
Ambient temperature;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
lithium azide in acetonitrile
20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
1: 64 percent / NEt3 / methanol; tetrahydrofuran / 1.17 h / -10 °C
2: 69 percent / NEt3 / methanol / Ambient temperature
View Scheme
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
1: 74 percent / O3/O2 / CH2Cl2 / 0.08 h / -78 °C
2: 64 percent / NEt3 / methanol; tetrahydrofuran / 1.17 h / -10 °C
3: 69 percent / NEt3 / methanol / Ambient temperature
View Scheme
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
参考文献
Miles Laboratories, Inc.
Patent: US3948929 A1, 1976 ;
反应条件
lithium azide in acetonitrile
20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
lithium azide in acetonitrile
20 h; Ambient temperature; Further byproducts given;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
1: hydrochloric acid, sodium nitrite / 0 °C
2: 28 percent / 60 h / Heating
View Scheme
参考文献
Hui, H. K.-W.; Shechter, H.
Tetrahedron Letters, 1982 , vol. 23, # 49 p. 5115 - 5118
