2-甲氧基-4-(甲基乙基)苯酚合成路线 （共 14 条）
参考文献
Saa, Jose M.; Morey, Jeronimo; Costa, Antonio
Tetrahedron Letters, 1986 , vol. 27, # 42 p. 5125 - 5128
反应条件
1: 1.) n-BuLi / 1.) THF,hexane, RT, 2.) from -40 deg C to 0 deg C 2: 63 percent / aq. HCl / tetrahydrofuran 3: 89 percent / PO4HNa2/PO4H2Na, Fremy's salt View Scheme
参考文献
Saa, Jose M.; Morey, Jeronimo; Costa, Antonio
Tetrahedron Letters, 1986 , vol. 27, # 42 p. 5125 - 5128
反应条件
1.1: n-BuLi / tetrahydrofuran / 4.25 h / -15 - 0 °C 1.2: tetrahydrofuran; CH2Cl2 / -10 °C 2.1: 14.5 g / DDQ / CH2Cl2; H2O / 2 h / 20 °C View Scheme
参考文献
Cook, Silas P.; Christoph, Gaul; Danishefsky, Samuel J.
Tetrahedron Letters, 2005 , vol. 46, # 5 p. 843 - 847
反应条件
toluene-4-sulfonic acid
T=20°C;
参考文献
THE TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK
Patent: WO2006/83417 A2, 2006 ;
Location in patent: Example 1 ;
反应条件
hydrogenchloride; sodium hydroxide in N-methyl-acetamide; methanol
参考文献
Otsuka Kagaku Yakuhin Kabushiki Kaisha
Patent: US4588835 A1, 1986 ;
反应条件
Mn(5,10,15,20-tetrakis(4-chlorophenyl)porphyrin)Cl; oxygen; sodium hydroxide in methanol
T=64.84°C; P=750.075 Torr; 3.5 h; Catalytic behavior; Reagent/catalystSolventTimeTemperature;
参考文献
Jiang, Qing; Sheng, Wenbing; Guo, Xiangdong; Tang, Jie; Guo, Cancheng
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 373, p. 121 - 126
反应条件
in methanol
0.0833333 h; Ambient temperature;
参考文献
Hazarika; Barua
Tetrahedron Letters, 1989 , vol. 30, # 47 p. 6567 - 6570
参考文献
Leopold
Svensk Papperstidning, 1952 , vol. 55, p. 816,819
反应条件
0.0833333 h; Ambient temperature;
参考文献
Hazarika; Barua
Tetrahedron Letters, 1989 , vol. 30, # 47 p. 6567 - 6570
反应条件
sodium tetrahydroborate
参考文献
Majumder, Suman; Majumder
Journal of the Indian Chemical Society, 2010 , vol. 87, # 12 p. 1539 - 1546
