3-羟基-2-甲基苯甲酸甲酯合成路线 (共 18 条)
反应条件
potassium hexamethylsilazane in N,N-dimethyl-formamide; toluene
参考文献
Warner-Lambert Company
Patent: US6133303 A1, 2000 ;
US 6133303 A
反应条件
potassium carbonate in acetone Etherification; Heating;
参考文献
Peixoto, Christophe; Laurin, Patrick; Klich, Michel; Dupuis-Hamelin, Claudine; Mauvais, Pascale; Lassaigne, Patrice; Bonnefoy, Alain; Musicki, Branislav
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1741 - 1745
反应条件
1: Br2 2: K2CO3 View Scheme
参考文献
Cresp,T.M. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 2435 - 2447
反应条件
1: Br2 2: K2CO3 3: aq. NaOH / methanol View Scheme
参考文献
Cresp,T.M. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 2435 - 2447
反应条件
1: Br2 2: K2CO3 View Scheme
参考文献
Cresp,T.M. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 2435 - 2447
参考文献
Fringuelli,F. et al.
Tetrahedron, 1969 , vol. 25, p. 4249 - 4256
反应条件
1: 72 percent / K2CO3 / acetone / Heating 2: 100 percent / LiAlH4 / diethyl ether / 20 °C View Scheme
参考文献
Peixoto, Christophe; Laurin, Patrick; Klich, Michel; Dupuis-Hamelin, Claudine; Mauvais, Pascale; Lassaigne, Patrice; Bonnefoy, Alain; Musicki, Branislav
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1741 - 1745
参考文献
Yamabe, Haruko; Okuyama, Masahiro; Nakao, Akira; Ooizumi, Mitsuru; Saito, Ken-ichi
Patent: US2003/212094 A1, 2003 ;
反应条件
hydrogenchloride
Esterification; Heating;
参考文献
Peixoto, Christophe; Laurin, Patrick; Klich, Michel; Dupuis-Hamelin, Claudine; Mauvais, Pascale; Lassaigne, Patrice; Bonnefoy, Alain; Musicki, Branislav
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1741 - 1745
反应条件
in methanol
T=0 - 20°C; 18 h;
参考文献
NOVO NORDISK A/S; Ontogen Corporation
Patent: EP1214324 B1, 2006 ;
Location in patent: Page/Page column 59-60 ;