Adlington, Robert M.; Barrett, Anthony G.M.; Quayle, Peter; Walker, Andrew; Betts, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 605 - 612
2: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min
3: 1.) n-butyl-lithium, 2.) toluene-4-sulphonyl chloride / 1.) THF, -78 deg -> 0 deg C, 2.) -78 deg C -> room temperature
View Scheme
参考文献
Adlington, Robert M.; Barrett, Anthony G.M.; Quayle, Peter; Walker, Andrew; Betts, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 605 - 612
2: 1.) n-butyl-lithium / 1.) DME, -78 deg C -> room temperature, 60 min, room temperature 30 min, 2.) -78 deg C -> room temperature 15 min
3: 1.) n-butyl-lithium, 2.) toluene-4-sulphonic anhydride / 1.) THF, -78 deg C -> 0 deg C, 2.) -78 deg C -> room temperature
View Scheme
参考文献
Adlington, Robert M.; Barrett, Anthony G.M.; Quayle, Peter; Walker, Andrew; Betts, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 605 - 612
