反应条件
1: 80 percent / sulfuric acid / acetic acid / 18 h / 20 °C
2: 1)1,1,1,3,3,3-hexamethyldisilazane 2)trimethylsilyl trifluormethanesulfonate / 1) pyridine, 2) 1,2-dichloroethane, 1.5 h, reflux
3: 79 percent / 5 M aqueous ammonia / methanol
View Scheme
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
