5,8-二甲氧基-1,4-二氢萘合成路线 （共 23 条）
参考文献
Zhurnal Obshchei Khimii, , vol. 15, p. 142,144
Chem.Abstr., , p. 1821
反应条件
(i), (ii) /BRN= 635994/; Multistep reaction;
参考文献
Archiv der Pharmazie, , vol. 310, # 5 p. 369 - 379
反应条件
1: 91 percent / m-CPBA / CH2Cl2 / 12 h / 20 °C 2: 42 percent / MgBr2*Et2O / toluene / 6 h / Heating View Scheme
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in xylene 12 h; Heating;
参考文献
Chemistry Letters, , vol. 32, # 12 p. 1190 - 1191
反应条件
1: sodium methylate; methanol / 130 °C
2: sodium; methanol
View Scheme
参考文献
Terentjew; Schawalowa
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 142,144
Chem.Abstr., 1946 , p. 1821
反应条件
1: 98 percent / potassium t-butoxide / dimethylsulfoxide / 6 h / Ambient temperature
2: 10 percent / POCl3 / CHCl3 / 4 h / Heating
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Sathaye, K. M.; Jaweed, S. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 697 - 702
反应条件
1: 98 percent / potassium t-butoxide / dimethylsulfoxide / 6 h / Ambient temperature
2: 10 percent / POCl3 / CHCl3 / 4 h / Heating
3: 90 percent / hydrogen / 5percent Pd/C / ethanol / 5 h / 1034.3 Torr / Ambient temperature
4: 1) potassium t-butoxide, O2, 2) gl. acetic acid, zinc dust / 1) t-butanol, 35 deg C, 5 min, 2) 6 h, r.t.
5: 70 percent / aluminium chloride, sodium chloride / 0.08 h / 180 °C
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Sathaye, K. M.; Jaweed, S. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 697 - 702
反应条件
1: 100 percent / tBuOK / dimethylsulfoxide / Ambient temperature
2: POCl3 / 4 h / 80 °C
View Scheme
参考文献
Rama Rao; Yadav; Bal Reddy; Mehendale
Tetrahedron, 1984 , vol. 40, # 22 p. 4643 - 4647
反应条件
potassium tert-butylate in dimethyl sulfoxide
Ambient temperature;
参考文献
Rao, A. V. Rama; Yadav, J. S.; Reddy, K. Bal; Mehendale, A. R.
Journal of the Chemical Society, Chemical Communications, 1984 , # 7 p. 453 - 455
参考文献
Terentjew; Schawalowa
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 142,144
Chem.Abstr., 1946 , p. 1821
