4-(2-羟基-2-丙基)环己烯-1-甲醇合成路线 （共 10 条）
反应条件
mercury(II) trifluoroacetate in tetrahydrofuran 24 h; Heating;
参考文献
Bull, Steven D.; Carman, Raymond M.; Carrick, Frank N.; Klika, Karel D.
Australian Journal of Chemistry, 1993 , vol. 46, # 4 p. 441 - 447
反应条件
5-chloro-1-methylimidazole; FeCl3·6H2O; dihydrogen peroxide in 1,1-dimethylpropan-1-ol; water
T=20°C; 1 h;
参考文献
Schroeder, Kristin; Junge, Kathrin; Spannenberg, Anke; Beller, Matthias
Catalysis Today, 2010 , vol. 157, # 1-4 p. 364 - 370
反应条件
1: 82 mg / N-bromosuccinimide / acetone; H2O / 1 h / Ambient temperature
2: NaOH / methanol / 0.08 h
3: p-TsOH / CH2Cl2 / 2 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
1: LiAlH4 / diethyl ether
2: 82 mg / N-bromosuccinimide / acetone; H2O / 1 h / Ambient temperature
3: NaOH / methanol / 0.08 h
4: p-TsOH / CH2Cl2 / 2 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
1: NaOH / methanol / 0.08 h
2: p-TsOH / CH2Cl2 / 2 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
1: 130 mg / NaOH / methanol / 0.08 h
2: p-TsOH / CH2Cl2 / 2 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
toluene-4-sulfonic acid in dichloromethane
2 h; Yield given. Yields of byproduct given;
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
toluene-4-sulfonic acid in dichloromethane
2 h; Yield given. Yields of byproduct given;
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
pyridine-2,6-dicarboxylic acid; N1,N1-Dimethyl-N2-cyclohexylformamidine; dihydrogen peroxide; iron
参考文献
Schroeder, Kristin; Enthaler, Stephan; Join, Benoit; Junge, Kathrin; Beller, Matthias
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1771 - 1778
反应条件
bei der Hydratation;
参考文献
Prileshajew; Prokoptschuk
Zhurnal Obshchei Khimii, 1933 , vol. 3, p. 866
Chem. Zentralbl., 1934 , vol. 105, # II p. 2368
Full Text Show Details
Prileshajew; Werschuk
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1929 , vol. 61, p. 463
Chem. Zentralbl., 1929 , vol. 100, # II p. 2556
