1-甲基-9H-芴-9-酮合成路线 （共 38 条）
反应条件
1.1: sodium carbonate / N,N-dimethyl-formamide; water / 0.08 h
1.2: 20 °C
2.1: tert.-butylhydroperoxide; biscyclopentadienyliron(II) / acetonitrile; decane / 24 h / 20 - 90 °C
View Scheme
参考文献
Wertz, Sebastian; Leifert, Dirk; Studer, Armido
Organic Letters, 2013 , vol. 15, # 4 p. 928 - 931
反应条件
1: KMnO4; acetone
2: Na2Cr2O7; acetic acid
3: quinoline; copper oxide-chromium oxide
View Scheme
参考文献
Mulholland; Ward
Journal of the Chemical Society, 1954 , p. 4676,4680
反应条件
1: N2H4+H2O; ethanolic sodium ethylate / 180 °C
2: Na2Cr2O7+2H2O; acetic acid
3: quinoline; copper oxide-chromium oxide
View Scheme
参考文献
Mulholland; Ward
Journal of the Chemical Society, 1954 , p. 4676,4680
参考文献
Haworth; Tinker
Journal of the Chemical Society, 1955 , p. 911,914
反应条件
quinoline; copper oxide-chromium oxide
参考文献
Mulholland; Ward
Journal of the Chemical Society, 1954 , p. 4676,4680
反应条件
1: Zn, aq. NH3 / ethanol
2: aq. HBr / acetic acid
View Scheme
参考文献
Gosnay,I. et al.
Israel Journal of Chemistry, 1972 , vol. 10, p. 423 - 437
反应条件
anhydrous ammonium carbonate; potassium cyanide in ethanol
参考文献
Alcon Laboratories, Inc.
Patent: US4540700 A1, 1985 ;
反应条件
(i), (ii) aq. H2SO4; Multistep reaction;
参考文献
Bonini,B.F. et al.
Gazzetta Chimica Italiana, 1975 , vol. 105, p. 827 - 839
