9 - (Β-D -呋喃核糖)嘌呤合成路线 (共 28 条)
反应条件
ammonia in ethanol 48 h; Ambient temperature;
参考文献
Nair; Chamberlain
Synthesis, 1984 , vol. NO. 5, p. 401 - 403
反应条件
Enterobacter gergoviae CECT 875 in agar in phosphate buffer T=60°C; pH=7.0; 3 h; Enzymatic reaction;
参考文献
Trelles; Fernandez; Lewkowicz; Iribarren; Sinisterra
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2605 - 2609
反应条件
ammonia in methanol T=4°C; 24 h;
参考文献
Gupta, P. K.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 534 - 537
反应条件
nickel in water Reduction; 6 h; Heating;
参考文献
Woerner, Karlheinz; Strube, Thorsten; Engels, Joachim W.
Helvetica Chimica Acta, 1999 , vol. 82, # 12 p. 2094 - 2104
反应条件
1: 69 percent / n-pentyl nitrite / tetrahydrofuran / 72 h / 50 °C 2: 77 percent / NaOMe View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 3 p. 462 - 470
反应条件
in dimethyl sulfoxide
参考文献
Dang, Qun; Liu, Yan; Erion, Mark D.
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5833 - 5834
反应条件
water; oxygen; copper(II) sulfate T=80°C; 6 h; Green chemistry;
参考文献
Xia, Ran; Xie, Ming-Sheng; Niu, Hong-Ying; Qu, Gui-Rong; Guo, Hai-Ming
Green Chemistry, 2014 , vol. 16, # 3 p. 1077 - 1081
反应条件
1: With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate in acetonitrile T=130°C; Vorbrueggen glycosylation; 0.0833333 h; microwave irradiation; 2: With ammonia in methanol T=50°C; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 1 p. 173 - 179
反应条件
1: 90.4 percent / Lawesson's reagent / pyridine / 6 h / Heating 2: 85.4 percent / NaOH / pyridine; methanol / 0.08 h / 20 °C 3: 79 percent / Raney-Ni / H2O / 6 h / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 82, # 12 p. 2094 - 2104
反应条件
1: 92.3 percent / pyridine / 4 h / 40 - 60 °C 2: 90.4 percent / Lawesson's reagent / pyridine / 6 h / Heating 3: 85.4 percent / NaOH / pyridine; methanol / 0.08 h / 20 °C 4: 79 percent / Raney-Ni / H2O / 6 h / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 82, # 12 p. 2094 - 2104