反应条件
1: 9.22 g / H2 / 5percent palladium-charcoal / ethyl acetate / 1.5 h / Ambient temperature
2: 1.) sodium ethoxide, 2.) 10percent methanolic potassium hydroxide / 1.) room temperature, 19 h, 2.) 22 h
3: 1.) oxalyl chloride / 1.) ether, 18 h
4: 42 mg / H2 / pre-reduced platinum oxide / ethanol / 1.25 h / Ambient temperature
View Scheme
参考文献
Pring, Brian G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1493 - 1498