2,2-二甲基-4-戊烯醛合成路线 （共 65 条）
反应条件
diisobutylaluminium hydride in pentane T=-78 - 20°C; 3 h;
参考文献
Yang, Jiong; Long, Yun Oliver; Paquette, Leo A.
Journal of the American Chemical Society, 2003 , vol. 125, # 6 p. 1567 - 1574
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78°C; 0.5 h;
参考文献
Chen, Guanghui; Ma, Xun S.; Guan, Zhibin
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6697 - 6704
反应条件
toluene-4-sulfonic acid in various solvent(s) 48 h; Heating;
参考文献
Magnus, P. D.; Nobbs, M. S.
Synthetic Communications, 1980 , vol. 10, # 4 p. 273 - 278
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide in tetrahydrofuran; water
参考文献
Block,E.; Ahmad,S.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6731
反应条件
potassium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
参考文献
Larock,R.C.; Oertle,K.; Potter,G.F.
Journal of the American Chemical Society, 1980 , vol. 102, p. 190
反应条件
oxalic acid in dichloromethane; water 2 h; Heating;
参考文献
De Kimpe, Norbert; De Smaele, Dirk; Hofkens, Arn; Dejaegher, Yves; Kesteleyn, Bart
Tetrahedron, 1997 , vol. 53, # 31 p. 10803 - 10816
参考文献
DiCosimo, Robert; Moore, Stephen S.; Sowinski, Allan F.; Whitesides, George M.
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 124 - 133
反应条件
phosphoric acid T=140°C;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 3379,3381
反应条件
1: 91 percent / LiAlH4 / diethyl ether / 3 h / Heating 2: 76 percent / oxalyl chloride; DMSO; Et3N / CH2Cl2 / 0.5 h / -78 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 22 p. 6697 - 6704
反应条件
water-d2 in phosphate buffer T=50°C; aza-Cope rearrangement; Kinetics; Further Variations:Reagents;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 48 p. 6748 - 6751
