2-氯-4-甲基-6-硝基喹啉合成路线 （共 9 条）
反应条件
trichlorophosphate in tetrahydrofuran
0.75 h; Heating;
参考文献
Heiskell, Melody R.; Rudd, Martin D.; Penn, Benjamin B.; Kautz, Jason A.
Synthetic Communications, 2005 , vol. 35, # 15 p. 2067 - 2077
反应条件
sulfuric acid; nitric acid
T=-5°C;
参考文献
Ishikawa; Kikkawa
Yakugaku Zasshi, 1955 , vol. 75, p. 33
Chem.Abstr., 1956 , p. 1007
Full Text Show Details
Adams; Hey
Journal of the Chemical Society, 1949 , p. 3185,3187
Full Text Show Details
Johnson; Hamilton
Journal of the American Chemical Society, 1941 , vol. 63, p. 2867
反应条件
in acetonitrile
T=130°C; 10 h;
参考文献
Lee, Byoung Se; Lee, Jae Hak; Chi, Dae Yoon
Journal of Organic Chemistry, 2002 , vol. 67, # 22 p. 7884 - 7886
反应条件
1: 90 percent / nitric acid; sulfuric acid / -5 - 20 °C
2: 90 percent / phosphorus oxychloride / tetrahydrofuran / 0.75 h / Heating
View Scheme
参考文献
Heiskell, Melody R.; Rudd, Martin D.; Penn, Benjamin B.; Kautz, Jason A.
Synthetic Communications, 2005 , vol. 35, # 15 p. 2067 - 2077
反应条件
1: H2O; K2CO3 / tetrahydrofuran / 12 h / Heating
2: 65 percent / acetonitrile / 10 h / 130 °C
View Scheme
参考文献
Lee, Byoung Se; Lee, Jae Hak; Chi, Dae Yoon
Journal of Organic Chemistry, 2002 , vol. 67, # 22 p. 7884 - 7886
反应条件
1: sulfuric acid
2: phosphoryl chloride
View Scheme
参考文献
Balaban
Journal of the Chemical Society, 1930 , p. 2346,2353
参考文献
Ishikawa; Kikkawa
Yakugaku Zasshi, 1955 , vol. 75, p. 33
Chem.Abstr., 1956 , p. 1007
参考文献
Kermack; Weatherhead
Journal of the Chemical Society, 1940 , p. 1164,1168
反应条件
titanium(III) chloride in acetone
Ambient temperature;
参考文献
Hayes, Roy; Schofield, Joseph M.; Smalley, Robert K.; Scopes, David I. C.
Tetrahedron, 1990 , vol. 46, # 6 p. 2089 - 2096
