1,1'-(苯基亚甲基)二(2,4,6-三甲氧基苯)合成路线 （共 19 条）
反应条件
FeCl3·6H2O in dichloromethane
T=0 - 20°C; Friedel Crafts arylation; 2.5 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
chloro-trimethyl-silane; bismuth sulphate
T=20°C; 1 h;
参考文献
Liu, Congrong; Li, Manbo
Chinese Journal of Chemistry, 2013 , vol. 31, # 10 p. 1274 - 1278
反应条件
iodine in methanol
T=20°C; aza-Friedel-Crafts reaction; 5 h;
参考文献
Jaratjaroonphong, Jaray; Krajangsri, Suppachai; Reutrakul, Vichai
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2476 - 2479
反应条件
chloro-trimethyl-silane; bismuth sulphate in dichloromethane
T=20°C; Friedel-Crafts reaction; 0.3 h;
参考文献
Liu, Cong-Rong; Li, Man-Bo; Yang, Cui-Feng; Tian, Shi-Kai
Chemical Communications, 2008 , # 10 p. 1249 - 1251
反应条件
1: amberlite H+ resin IR-120 / toluene / 12 h / 120 °C / |Dean-Stark; |Molecular sieve
2: [Ir(COD)(SnCl3)Cl(μ-Cl)]2 / 1,2-dichloro-ethane / 0.67 h / 20 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Chatterjee, Paresh Nath; Maity, Arnab Kumar; Mohapatra, Swapna Sarita; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 13 p. 2816 - 2826
反应条件
ethanol; benzene
Irradiation.UV-Licht;
参考文献
Lifschitz
Z. wiss. Phot., 1930 , vol. 29, p. 91,98
参考文献
v. Kostanecki; Lampe
Chemische Berichte, 1906 , vol. 39, p. 4017
反应条件
1: POCl3; diethyl ether / anschliessend Behandeln des Reaktionsprodukts mit wss. NaOH
3: acetic acid; aqueous H2SO4
View Scheme
参考文献
Kenyon; Mason
Journal of the Chemical Society, 1952 , p. 4964,4966
反应条件
2: acetic acid; aqueous H2SO4
View Scheme
参考文献
Kenyon; Mason
Journal of the Chemical Society, 1952 , p. 4964,4966
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
