1-(4-氨基-3-羟基苯基)-乙酮(9ci)合成路线 (共 5 条)
反应条件
sodium hydroxide
4 h; Heatingother 6-acyl-2(3H)-benzoxazolinones;
参考文献
Aichaoui, Hocine; Lesieur, Isabelle; Henichart, Jean-Pierre
Synthesis, 1990 , # 8 p. 679 - 680
反应条件
1: hydrogenchloride / water / 150 °C
2: polyphosphoric acid / 3 h / 90 - 100 °C
3: water; sodium hydroxide / 6 h / Reflux
View Scheme
参考文献
Bali, Alka; Ohri, Ruchika; Deb, Pran Kishore
European Journal of Medicinal Chemistry, 2012 , vol. 49, p. 397 - 405
反应条件
1: polyphosphoric acid / 3 h / 90 - 100 °C
2: water; sodium hydroxide / 6 h / Reflux
View Scheme
参考文献
Bali, Alka; Ohri, Ruchika; Deb, Pran Kishore
European Journal of Medicinal Chemistry, 2012 , vol. 49, p. 397 - 405
参考文献
Butenandt et al.
Chemische Berichte, 1959 , vol. 92, p. 2172,2174
反应条件
sodium hydrogencarbonate in water
参考文献
Baldwin; John J.; Atkinson; Joseph; McClure; David E.
Patent: US4816457 A1, 1989 ;
US 4816457 A