[(2-苯基乙氧基)甲基]苯合成路线 (共 34 条)
反应条件
carbon monoxide; oxygen; copper dichloride; palladium dichloride in acetone P=45600 Torr; 48 h;
参考文献
Miyamoto, Masanori; Minami, Yumiko; Ukaji, Yutaka; Kinoshita, Hideki; Inomata, Katsuhiko
Chemistry Letters, 1994 , # 7 p. 1149 - 1152
反应条件
indium(III) chloride; silica gel 0.25 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Samanta, Sampak; Hajra, Alakananda
Synlett, 2002 , # 6 p. 987 - 989
反应条件
1: Ph(CH2)2OBn With 1-bromo-1,1-dimethylethane; [C5mim](+)*Br(-) T=60°C; 2: thiophenol With [C5mim](+)*Br(-) T=60°C; Title compound not separated from byproducts;
参考文献
Ranu, Brindaban C.; Jana, Ranjan
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 14 p. 1811 - 1818
反应条件
nitric acid in dichloromethane T=20°C; 1 h;
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
lithium bromide in dichloromethane T=30 - 35°C; 6 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 3 p. 1367 - 1370
反应条件
1: Ph(CH2)2OBn With 1-bromo-1,1-dimethylethane; [C5mim](+)*Br(-) T=60°C; 2: thiophenol With [C5mim](+)*Br(-) T=60°C; Title compound not separated from byproducts;
参考文献
Ranu, Brindaban C.; Jana, Ranjan
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 14 p. 1811 - 1818
反应条件
1: With chlorosulphonyl isocyanate; sodium carbonate in dichloromethane 20 h; Heating; 2: With sodium hydroxide in methanol T=20°C; 1 h;
参考文献
Cheng, Lili; Aw, Carlin; Ong, Siew Siang; Lu, Yixin
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 10 p. 2008 - 2010
参考文献
Baker; Cornell; Cron
Journal of the American Chemical Society, 1948 , vol. 70, p. 1490
反应条件
1: 2-phenyl-ethanol With sodium hydride in tetrahydrofuran
T=0°C; 0.5 h; Inert atmosphere;
2: benzyl bromide in tetrahydrofuran
T=0 - 20°C;
参考文献
Chakraborti, Asit K.; Chankeshwara, Sunay V.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1367 - 1370
反应条件
n-butyllithium; 2,3,5,6-tetrafluoro-1,4-benzoquinone in dichloromethane
T=20°C; 3 h;
参考文献
Shintou, Taichi; Mukaiyama, Teruaki
Journal of the American Chemical Society, 2004 , vol. 126, # 23 p. 7359 - 7367