3-(七氟正丙基)-5-苯基吡唑合成路线 （共 5 条）
反应条件
hydrogenchloride; hydrazine in methanol
T=60°C; 3 h; Heating;
参考文献
Peglion, Jean-Louis; Pastor, Raphael-Emile; Cambon, Aime-Roger
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 309 - 315
反应条件
hydrazine hydrate in ethanol
2 h; Heating;
参考文献
Tang, Xiao-Qing; Hu, Chang-Ming
Journal of Fluorine Chemistry, 1995 , vol. 73, # 2 p. 129 - 132
反应条件
1: With oxygen; 1,1,1,2,2,2-hexabutyl-distannane in benzene
5 h; Irradiation;
2: With hydrazinium monoacetate in ethanol
2 h; Heating;
参考文献
Ohkoshi, Masanori; Yoshida, Masato; Matsuyama, Haruo; Iyoda, Masahiko
Tetrahedron Letters, 2001 , vol. 42, # 1 p. 33 - 36
反应条件
1: 74 percent / NaH / diethyl ether
2: 86 percent / hydrazine, cc. HCl / methanol / 3 h / 60 °C / Heating
View Scheme
参考文献
Peglion, Jean-Louis; Pastor, Raphael-Emile; Cambon, Aime-Roger
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 309 - 315
反应条件
bromine; sodium acetate in chloroform
24 h; Ambient temperature;
参考文献
Peglion, Jean-Louis; Pastor, Raphael; Greiner, Jaques; Cambon, Aime
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 1-2 p. 89 - 94
