(Z)-6-二十一碳烯-11-酮合成路线 （共 124 条）
反应条件
hydrogenchloride in diethyl ether 2.5 h; Ambient temperature;
参考文献
Dhillon, Ranjit S.; Singh, Swaranjit; Singh, Jasvinder
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 4 p. 365 - 367
反应条件
1: 1.15 g / triethylamine / CH2Cl2 / 0 °C 2: 1.25 g / sodium iodide / acetone / 3 h / Heating 3: 90 percent / sodium hydride, DMSO / diethyl ether / 2.5 h / Ambient temperature 4: 100 percent / conc. HCl / CH2Cl2; diethyl ether / 0.17 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 13, # 5 p. 379 - 386
反应条件
potassium fluoride in methanol T=30°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 50, # 25 p. 5260 - 5267
反应条件
1: 91 percent / aq. HCl / acetone / 1 h / Heating 2: 95 percent / H2, NaBH4, Ni(CH3COO)2*4H2O, NH2(CH2)2NH2 / ethanol View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 11.1 p. 1750 - 1753
Zhurnal Organicheskoi Khimii, , vol. 30, # 11 p. 1664 - 1666
反应条件
1: 1.) n-BuLi 4: 1.) NaH / 1.) THF 5: 88 percent / H2 / naphthalenetricarbonylchromium / tetrahydrofuran / 8 h / 45 °C / 36775.4 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1147 - 1149
反应条件
3: 1.) NaH / 1.) THF 4: 88 percent / H2 / naphthalenetricarbonylchromium / tetrahydrofuran / 8 h / 45 °C / 36775.4 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1147 - 1149
反应条件
2: 1.) NaH / 1.) THF 3: 88 percent / H2 / naphthalenetricarbonylchromium / tetrahydrofuran / 8 h / 45 °C / 36775.4 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1147 - 1149
反应条件
1: 1.) NaH / 1.) THF 2: 88 percent / H2 / naphthalenetricarbonylchromium / tetrahydrofuran / 8 h / 45 °C / 36775.4 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1147 - 1149
反应条件
in tetrahydrofuran T=-78°C; 3 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 691 - 692
反应条件
potassium tert-butylate in tetrahydrofuran
参考文献
Dasaradhi, L.; Bhalerao, U. T.
Synthetic Communications, 1987 , vol. 17, # 15 p. 1845 - 1850
