反应条件
1: 1) NaH / 1) THF, hexane, rt, 2 h, 2) THF, rt, overnight 2: m-chloroperbenzoic acid / acetone / 4 h / Ambient temperature 3: 2) Me2NCOCl / 1) CH2Cl2, 5 min, rt, 2) rt, overnight 4: 76 percent / 6 N HCl / Heating View Scheme
参考文献
Ornstein, Paul L.; Schaus, John M.; Chambers, John W.; Huser, Diane L.; Leander, J. David; et al.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 4 p. 827 - 833
