反应条件
1: With (η5-cyclopentadienyl)dicarbonyl(1,3-dimesityl-5-tert-butyl-6-oxo-6H-pyrimidin-2-ylidene-4-olate)iron(II); (Ph)2SiH2 in tetrahydrofuran
T=30°C; 3 h; Inert atmosphereSchlenk techniqueIrradiation;
2: With water; sodium hydroxide in tetrahydrofuran; methanol
T=20°C; 2 h;
参考文献
Cesar, Vincent; Misal Castro, Luis C.; Dombray, Thomas; Sortais, Jean-Baptiste; Darcel, Christophe; Labat, Stephane; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Brousses, Remy; Lugan, Noel; Lavigne, Guy
Organometallics, 2013 , vol. 32, # 16 p. 4643 - 4655