2-氨基-4’-甲氧基苯乙酮盐酸盐合成路线 （共 10 条）
反应条件
hydrogen; sulfided platinum on carbon in hydrogenchloride; ethanol T=50°C; P=760 Torr; 11.5 h;
参考文献
Tamura, Rui; Oda, Daihei; Kurokawa, Hiroshi
Tetrahedron Letters, 1986 , vol. 27, # 47 p. 5759 - 5762
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol; diethyl ether T=20°C; P=2250.23 Torr; 5 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 27 p. 7780 - 7784
反应条件
hydrogenchloride; ethanol 48 h; Ambient temperature;
参考文献
Yinglin, Han; Hongwen, Hu
Synthesis, 1990 , # 7 p. 615 - 618
参考文献
Maeda; Suzuki; Iwasaki; Matsumoto; Iwasawa
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2536 - 2543
反应条件
1: 90 percent / acetonitrile / 2 h / Ambient temperature 2: 5percent HCl / ethanol / 48 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 39 p. 5285 - 5286
反应条件
hydrogenchloride 1a) EtOH, RT, 2h, 1b) 50 deg C, 30 min, 2) 30 min, reflux; Yield given. Multistep reaction;
参考文献
Synthesis, , # 7 p. 615 - 618
反应条件
1: 76 percent / HCl 2: 94 percent / HCl View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 7 p. 2536 - 2543
反应条件
1: 10percent aq. Na2CO3 / benzene; H2O / 1 h / 25 °C 2: conc. H2SO4 / 2 h / 25 °C 3: 80 percent / aq. NaOH / acetone / 3 h / Heating 4: SOCl2 5: 96 percent / 10percent aq. NH3 / benzene / 20 °C View Scheme
参考文献
Krasovitskii, B. M.; Shershukov, V. M.; Volkov, V. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 9 p. 1022 - 1025
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 9 p. 1261 - 1264
反应条件
hydrogen; potassium carbonate; [Rh(R,R,S,S-DuanPhos)(nbd)]SbF6 in 2,2,2-trifluoroethanol T=20°C; P=7600.51 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Shang, Gao; Liu, Duan; Allen, Scott E.; Yang, Qin; Zhang, Xumu
Chemistry - A European Journal, 2007 , vol. 13, # 27 p. 7780 - 7784
反应条件
sodium tetrahydroborate in methanol
T=0°C; 0.5 h;
参考文献
Shang, Gao; Liu, Duan; Allen, Scott E.; Yang, Qin; Zhang, Xumu
Chemistry - A European Journal, 2007 , vol. 13, # 27 p. 7780 - 7784
