N-(3-溴丙基)苯二胺合成路线 （共 93 条）
反应条件
hydrazine hydrate
Multistep reaction;
参考文献
He, Xiao Shu; Woodruff, Kristine; Brodbeck, Robbin
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 18 p. 2399 - 2402
反应条件
T=100°C; Man kocht das Reaktionsprodukt mit 15prozentiger Natronlauge und erhitzt danach mit gesaettigter Salzsaeure im Rohr auf 100grad;
参考文献
Wrede; Fanselow; Strack
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1927 , vol. 163, p. 225
反应条件
trisodium phosphorothioate in N,N-dimethyl-formamide
5 h;
参考文献
Bieniarz; Cornwell
Tetrahedron Letters, 1993 , vol. 34, # 6 p. 939 - 942
反应条件
[Ni0(1,5-cyclooctadiene)2]; zinc; (4-Cl)-H-PyBox in N,N-dimethyl acetamide
T=25°C; 16 h; Inert atmosphere;
参考文献
Yu, Xiaolong; Yang, Tao; Wang, Shulin; Xu, Hailiang; Gong, Hegui
Organic Letters, 2011 , vol. 13, # 8 p. 2138 - 2141
反应条件
hypophosphorous acid; triethylamine; Vazo44 in isopropyl alcohol
T=80°C; 0.5 h;
参考文献
Nambu, Hisanori; Alinejad, Anahita Hessamian; Hata, Kayoko; Fujioka, Hiromichi; Kita, Yasuyuki
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8927 - 8929
反应条件
in dimethyl sulfoxide
T=25°C;
参考文献
Martin, David P.; Bibart, Richard T.; Drueckhammer, Dale G.
Journal of the American Chemical Society, 1994 , vol. 116, # 11 p. 4660 - 4668
反应条件
sodium methylate in methanol
参考文献
McElhinney, R. Stanley; McCormick, Joan E.; Bibby, Mike C.; Double, John A.; Radacic, Marco; Dumont, Patrick
Journal of Medicinal Chemistry, 1996 , vol. 39, # 7 p. 1408 - 1412
参考文献
Schneider
Justus Liebigs Annalen der Chemie, 1910 , vol. 375, p. 248
参考文献
Erickson, Shawn David; Baldwin, John J.; Dolle III, Roland Ellwood; Inglese, James; Ohlmeyer, Michael H.J.; Ho, Koc-Kan; Bohnstedt, Adolph C.; Kultgen, Steven G.; Conti, Paolo Giovanni Martino; Leysen, Dirk; van der Louw, Jaap
Patent: US2004/87601 A1, 2004 ;
Location in patent: Page 26 ;
US 20040087601 A1
反应条件
triethylamine in tetrahydrofuran; hydrogenchloride
参考文献
Zaidan Hojin Biseibutsu Kagaku Kenkyu Kai
Patent: US4537880 A1, 1985 ;
