N-(3-溴丙基)苯二胺合成路线 （共 93 条）
反应条件
1: 100 percent / NaI / acetone / 14 h / Heating
2: 48 percent / Pd2(dba)3; PCyp3; N-methylimidazole / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 14 h / 80 °C
View Scheme
参考文献
Zhou, Jianrong; Fu, Gregory C.
Journal of the American Chemical Society, 2003 , vol. 125, # 41 p. 12527 - 12530
反应条件
methanol; sodium methylate
und Erwaermen des Reaktionsprodukts mit wss.-methanol.Salzsaeure;
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
参考文献
Manka; Lawrence
Journal of the American Chemical Society, 1990 , vol. 112, # 6 p. 2440 - 2442
参考文献
Barber; Wragg
Journal of the Chemical Society, 1947 , p. 1332
参考文献
Glen; Robinson
Journal of the Chemical Society, 1943 , p. 557,558
Show Details
Quin; Robinson
Journal of the Chemical Society, 1943 , p. 555
参考文献
Gerpe, Alejandra; Bollini, Mariela; Gonzalez, Mercedes; Cerecetto, Hugo
Synthetic Communications, 2009 , vol. 39, # 1 p. 29 - 47
反应条件
sodium nitrite in dimethyl sulfoxide
0.5 h;
参考文献
Hughes, Robert; Prager, Rolf H.
Australian Journal of Chemistry, 1997 , vol. 50, # 1 p. 19 - 26
反应条件
sodium carbonate in acetonitrile
T=80°C; Alkylation; 48 h;
参考文献
Quici, Silvio; Manfredi, Amedea; Pozzi, Gianluca; Cavazzini, Marco; Rozzoni, Angela
Tetrahedron, 1999 , vol. 55, # 34 p. 10487 - 10496
参考文献
Cho, Iwhan; Chang, Suk-Kyu
Chemistry Letters, 1981 , p. 515 - 518
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=90°C; 4 h;
参考文献
Thorat, Dhanaji Achyutrao; Doddareddy, Munikumar Reddy; Seo, Seon Hee; Hong, Tae-Joon; Cho, Yong Seo; Hahn, Ji-Sook; Pae, Ae Nim
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 6 p. 1593 - 1597
