(1E)-N-羟基-1-(4-甲基苯基)乙烷亚胺合成路线 （共 12 条）
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in ethylene glycol dimethyl ether T=20°C; 40 h; 2: With hydrogenchloride in methanol; ethylene glycol dimethyl ether Further stages. Title compound not separated from byproducts.;
参考文献
Takei; Nishibayashi; Ishii; Mizobe; Uemura; Hidai
Chemical Communications, 2001 , # 22 p. 2360 - 2361
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in ethylene glycol dimethyl ether T=20°C; 40 h; 2: With hydrogenchloride in methanol; ethylene glycol dimethyl ether Further stages. Title compound not separated from byproducts.;
参考文献
Takei; Nishibayashi; Ishii; Mizobe; Uemura; Hidai
Chemical Communications, 2001 , # 22 p. 2360 - 2361
反应条件
perchloric acid; Chrome in water; N,N-dimethyl-formamide T=30°C; Rate constantMechanism;
参考文献
Journal of the Indian Chemical Society, , vol. 65, p. 404 - 406
反应条件
T=120°C; Beckmann rearrangement; 1.5 h; Heating;
参考文献
Zhu, Minze; Cha, Chuantao; Deng, Wei-Ping; Shi, Xiao-Xin
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4861 - 4863
参考文献
Pearson; Ball
Journal of Organic Chemistry, 1949 , vol. 14, p. 118,121, 128
反应条件
1: NaH / dimethylformamide / 20 °C 2: borane; NaBH4 / enantiopure spiroborate ester / dioxane / 36 h View Scheme
参考文献
Huang, Xiaogen; Ortiz-Marciales, Margarita; Huang, Kun; Stepanenko, Viatcheslav; Merced, Francisco G.; Ayala, Angel M.; Correa, Wildeliz; De Jesus, Melvin
Organic Letters, 2007 , vol. 9, # 9 p. 1793 - 1795
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in ethylene glycol dimethyl ether T=20°C; 40 h; 2: With hydrogenchloride in methanol; ethylene glycol dimethyl ether Further stages. Title compound not separated from byproducts.;
参考文献
Takei; Nishibayashi; Ishii; Mizobe; Uemura; Hidai
Chemical Communications, 2001 , # 22 p. 2360 - 2361
参考文献
Stephen; Bleloch
Journal of the Chemical Society, 1931 , p. 886,887, 894
反应条件
hydroxylamine hydrochloride; sodium acetate in methanol
Heating;
参考文献
Augustine, John Kallikat; Kumar, Rajesha; Bombrun, Agnes; Mandal, Ashis Baran
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1074 - 1077
反应条件
hydroxylamine in 1,4-dioxane; water
T=113°C; intermolecular Cope-type hydroamination;
参考文献
Beauchemin, Andre M.; Moran, Joseph; Lebrun, Marie-Eve; Seguin, Catherine; Dimitrijevic, Elena; Zhang, Lili; Gorelsky, Serge I.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 8 p. 1410 - 1413
