2-(4-碘丁基)异吲哚-1,3-二酮合成路线 （共 12 条）
反应条件
toluene Beim Erhitzen des Reaktionsprodukts mit Essigsaeure und wss. HCl;
参考文献
Arnstein et al.
Journal of the Chemical Society, 1952 , p. 1329,1331
Org. Synth. Isotopes, 1958 , p. 274
反应条件
toluene Beim Erhitzen des Reaktionsprodukts mit Essigsaeure und wss. HCl;
参考文献
Arnstein et al.
Journal of the Chemical Society, 1952 , p. 1329,1331
Org. Synth. Isotopes, 1958 , p. 274
反应条件
acetone; sodium iodide
参考文献
Fields et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1000
反应条件
sodium iodide in acetone
2 h; Heating;
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
1: 88 percent / dimethylsulfoxide / 2 h / 65 °C
2: 54.5 percent / H2, HCl conc. / PtO2 / ethanol / 24 h / 2327.2 Torr
3: 87.6 percent / Et3N / CH2Cl2 / 4 h
4: 96 percent / NaNO2 / acetic acid; acetic anhydride / 4 °C
5: 54 percent / Na2CO3 / CCl4 / 40 h / Heating
6: 90.4 percent / NaI / acetone / 2 h / Heating
View Scheme
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
1: 54.5 percent / H2, HCl conc. / PtO2 / ethanol / 24 h / 2327.2 Torr
2: 87.6 percent / Et3N / CH2Cl2 / 4 h
3: 96 percent / NaNO2 / acetic acid; acetic anhydride / 4 °C
4: 54 percent / Na2CO3 / CCl4 / 40 h / Heating
5: 90.4 percent / NaI / acetone / 2 h / Heating
View Scheme
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
1: 96 percent / NaNO2 / acetic acid; acetic anhydride / 4 °C
2: 54 percent / Na2CO3 / CCl4 / 40 h / Heating
3: 90.4 percent / NaI / acetone / 2 h / Heating
View Scheme
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
1: 54 percent / Na2CO3 / CCl4 / 40 h / Heating
2: 90.4 percent / NaI / acetone / 2 h / Heating
View Scheme
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
反应条件
1: K2CO3, n-Bu4NBr / acetone / 24 h / Ambient temperature
2: NaI / acetone / Ambient temperature
View Scheme
参考文献
Ha, Deok-Chan; Yun, Chang-Soo; Yu, Eunsun
Tetrahedron Letters, 1996 , vol. 37, # 15 p. 2577 - 2580
反应条件
acetone; sodium iodide
参考文献
Arnstein et al.
Journal of the Chemical Society, 1952 , p. 1329,1331
Org. Synth. Isotopes, 1958 , p. 274
