N-N-丁基-4-甲基苯甲酰胺合成路线 （共 17 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane; bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine in tetrahydrofuran
T=25°C; P=760.051 Torr; 12 h;
参考文献
Uozumi; Arii; Watanabe
Journal of Organic Chemistry, 2001 , vol. 66, # 15 p. 5272 - 5274
反应条件
tert.-butylhydroperoxide; potassium iodide in water
T=80°C; 15 h;
参考文献
Rajender Reddy; Uma Maheswari; Venkateshwar; Lakshmi Kantam
European Journal of Organic Chemistry, 2008 , # 21 p. 3619 - 3622
反应条件
palladium diacetate; triethylamine in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Tambade, Pawan J.; Patil, Yogesh P.; Bhanushali, Mayur J.; Bhanage, Bhalchandra M.
Synthesis, 2008 , # 15 art. no. P04608SS, p. 2347 - 2352
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Sather, Aaron C.; Berryman, Orion B.; Ajami, Dariush; Rebek Jr., Julius
Tetrahedron Letters, 2011 , vol. 52, # 17 p. 2100 - 2103
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine; trichlorophosphate in dichloromethane
T=20°C; 2 h;
参考文献
Chen, Hu; Xu, Xunfu; Liu, Liu; Tang, Guo; Zhao, Yufen
RSC Advances, 2013 , vol. 3, # 37 p. 16247 - 16250
反应条件
sodium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in water
T=170°C; 0.166667 h; microwave irradiation;
参考文献
Wu, Xiongyu; Larhed, Mats
Organic Letters, 2005 , vol. 7, # 15 p. 3327 - 3329
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
in chloroform
T=80°C; 0.166667 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Singh, Sandeep K.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3375 - 3380
反应条件
1: 95 percent / SOCl2 / CH2Cl2 / 20 °C
2: 92 percent / CHCl3 / 0.17 h / 80 °C / microwave irradiation
View Scheme
参考文献
Katritzky, Alan R.; Cai, Chunming; Singh, Sandeep K.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3375 - 3380
反应条件
1: tert.-butylhydroperoxide; copper (II) acetate monohydrate / water; acetonitrile / 0.67 h / |Inert atmosphere; |Reflux
2: water; acetonitrile / 0.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Pilo, Monica; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8241 - 8246
