N-(2,3-环氧丙基)邻苯二甲酰胺合成路线 (共 23 条)
反应条件
in ethylene glycol dimethyl ether T=120°C; 3 h;
参考文献
Kirin Beer Kabushiki Kaisha
Patent: US6875884 B1, 2005 ;
Location in patent: Page/Page column 26; 203-204 ;
US 6875884 B1
参考文献
Meyer, Joerg; Keul, Helmut; Moeller, Martin
Macromolecules, 2011 , vol. 44, # 11 p. 4082 - 4091
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Carruthers, Nicholas I.; Spitler, James M.; Wong, Shing-Chun; Blythin, David J.; Chen, Xiao; Shue, Ho-Jane; She, Hoyan S.; Lee, Joe F.; Rizzo, Charles; Ting, Pauline C.; West Jr., Robert E.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 21 p. 3059 - 3064
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran Mitsunobu reaction;
参考文献
Ishige, Hirohide; Ishiyama, Nobuo; Mimura, Mitsuo; Hayashida, Mitsuo; Okuno, Tadashi; Ukai, Kiyoharu; Kiyofuji, Takeshi; Yoneda, Yasuo; Tauchi, Shinji; Aoyama, Akinori; Inoguchi, Kiyoshi
Heterocycles, 2006 , vol. 67, # 2 p. 561 - 566
反应条件
potassium fluoride supported on Celite in acetonitrile 0.5 h; Reflux; regioselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Sinisterra, Jose Vicente; Alcantara, Andres R.; Holzer, Wolfgang
Synlett, 2011 , # 13 p. 1831 - 1834
反应条件
potassium fluoride; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=85°C; 6 h;
参考文献
Hu, Yi; Chen, Zhen-Chu; Le, Zhang-Gao; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 4 p. 276 - 278
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran 3 h; Inert atmosphereReflux; chemoselective reaction;
参考文献
Green Chemistry, , vol. 12, # 8 p. 1380 - 1382
反应条件
1: 80.2 percent / dimethylformamide / 50 °C 2: 92 percent / m-chloroperbenzoic acid / CH2Cl2 / 72 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 1 p. 99 - 114
参考文献
US5663173 A1, ;
US 5663173 A
反应条件
dicobalt octacarbonyl T=20°C; P=760.051 Torr; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9630 - 9634