2-苯基氨基亚甲基-丙二酸二乙酯合成路线 (共 32 条)
反应条件
1: allyl bromide With indium in tetrahydrofuran T=20°C; 1 h; 2: aniline; diethyl 2-ethoxymethylenemalonate in tetrahydrofuran 2 h;
参考文献
Organic Letters, , vol. 8, # 2 p. 195 - 198
反应条件
in ethanol T=28°C; 0.333333 h;
参考文献
Chemistry - A European Journal, , vol. 16, # 9 p. 2938 - 2943
反应条件
1: ethanol / 5 h / Heating 2: H2 / Raney-Ni / ethanol / Ambient temperature 3: diethyl ether / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 104, p. 715 - 729
反应条件
PEG-400; potassium carbonate in acetonitrile Heating;
参考文献
Synthetic Communications, , vol. 29, # 10 p. 1801 - 1809
反应条件
1: ethanol / 5 h / Heating 2: H2 / Raney-Ni / ethanol / Ambient temperature 3: diethyl ether / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 104, p. 715 - 729
反应条件
1: H2 / Raney-Ni / ethanol / Ambient temperature 2: diethyl ether / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 104, p. 715 - 729
反应条件
1: 90 percent / acetonitrile / Heating 2: 82 percent / K2CO3, PEG-400 / acetonitrile / Heating View Scheme
参考文献
Synthetic Communications, , vol. 29, # 10 p. 1801 - 1809
反应条件
1: 97 percent / Ac2O, montmorillonite KF-10 / 5 h / 140 - 150 °C 2: 90 percent / acetonitrile / Heating 3: 82 percent / K2CO3, PEG-400 / acetonitrile / Heating View Scheme
参考文献
Synthetic Communications, , vol. 29, # 10 p. 1801 - 1809
反应条件
acetic anhydride; zinc(II) chloride 1.) reflux, 5 h, 2.) reflux, 30 min; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 17, # 5 p. 549 - 554
反应条件
1: diethyl ether 2: water View Scheme
参考文献
Chemische Berichte, , vol. 30, p. 1757