hydrogen; palladium on activated charcoal in water; acetic acid; isopropyl alcohol
T=20°C; 120 h;
参考文献
Dalmolen, Jan; Van Der Sluis, Marcel; Nieuwenhuijzen, Jose W.; Meetsma, Auke; De Lange, Ben; Kaptein, Bernard; Kellogg, Richard M.; Broxterman, Quirinus B.
European Journal of Organic Chemistry, 2004 , # 7 p. 1544 - 1557
1: 85 percent / CH2Cl2 / 20 °C
2: 89 percent / tetrahydrofuran / 0 - 20 °C
3: H2 / Pd/C / propan-2-ol; H2O; acetic acid / 120 h / 20 °C
View Scheme
参考文献
Dalmolen, Jan; Van Der Sluis, Marcel; Nieuwenhuijzen, Jose W.; Meetsma, Auke; De Lange, Ben; Kaptein, Bernard; Kellogg, Richard M.; Broxterman, Quirinus B.
European Journal of Organic Chemistry, 2004 , # 7 p. 1544 - 1557
1: 89 percent / tetrahydrofuran / 0 - 20 °C
2: H2 / Pd/C / propan-2-ol; H2O; acetic acid / 120 h / 20 °C
View Scheme
参考文献
Dalmolen, Jan; Van Der Sluis, Marcel; Nieuwenhuijzen, Jose W.; Meetsma, Auke; De Lange, Ben; Kaptein, Bernard; Kellogg, Richard M.; Broxterman, Quirinus B.
European Journal of Organic Chemistry, 2004 , # 7 p. 1544 - 1557
Wittig; Pohmer
Chemische Berichte, 1956 , vol. 89, p. 1334,1348
Full Text Show Details
Huisgen; Zirngibl
Chemische Berichte, 1958 , vol. 91, p. 1438,1451
