1,3-二(4-溴苯基)丙酮合成路线 （共 11 条）
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
参考文献
Doklady Chemistry, , vol. 442, # 2 p. 23 - 29
反应条件
pentacarbonyliron(0); tetra-n-butyl-ammonium sulfate in sodium hydroxide; dichloromethane T=25°C; P=760 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 24, # 37 p. 4005 - 4008
反应条件
in various solvent(s) T=0 - 50°C;
参考文献
Organic Letters, , vol. 9, # 7 p. 1187 - 1190
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.75 h;
参考文献
Chemistry Letters, , p. 25 - 28
反应条件
1: With tetra-(n-butyl)ammonium iodide; sodium hydroxide in dichloromethane; water 4 h; 2: With hydrogenchloride; water in dichloromethane T=20°C; 4 h;
参考文献
Synlett, , # 9 p. 1293 - 1295
反应条件
calcium hydroxide powder in dichloromethane; water T=20°C; 23 h;
参考文献
Tetrahedron Letters, , vol. 25, # 48 p. 5529 - 5532
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3224,3226
反应条件
hydrogenchloride; lithium diisopropyl amide 1a) ether, 0 deg C, 15 min, 1b) up to r.t., 20 h, 2) glac.HOAc, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 56, # 2 p. 688 - 694
反应条件
1: 4-bromo-benzyl bromide With tetra(n-butyl)ammonium hydrogensulfate; Ca(OH)2 in dichloromethane; water 0.25 h; Inert atmosphere; 2: pentacarbonyliron(0) in dichloromethane; water Inert atmosphere;
参考文献
Crystal Growth and Design, , vol. 10, # 5 p. 2298 - 2305
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether Suzuki coupling;
参考文献
Thiemann, Thies; Iniesta, Jesus; Walton, David J.
Journal of Chemical Research, 2008 , # 3 p. 173 - 180
