2,4'-二甲氧基二苯甲酮合成路线 （共 25 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; Molecular sieve;
参考文献
TFCHEM; DELIENCOURT-GODEFROY, Geraldine; LOPES, Lenaig
Patent: WO2012/160218 A1, 2012 ;
Location in patent: Page/Page column 59 ;
WO 2012/160218 A1
反应条件
potassium carbonate; [(t-Bu)3PH]BF4; [Rh(C2H4)2Cl]2 in 1,4-dioxane; acetone T=80°C;
参考文献
Chuzel, Olivier; Roesch, Alexander; Genet, Jean-Pierre; Darses, Sylvain
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7800 - 7802
反应条件
tris-(o-tolyl)phosphine; palladium diacetate in toluene T=20°C; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 2 p. 331 - 340
反应条件
N,N,N',N,-tetramethylethylenediamine; α-n-hexadecene; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; Suzuki reaction; P=3750.38 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Neumann, Helfried; Brennfuehrer, Anne; Beller, Matthias
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3645 - 3652
反应条件
potassium phosphate; platinacycle; pentan-3-one in toluene T=90 - 100°C;
参考文献
Liao, Yuan-Xi; Hu, Qiao-Sheng
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6986 - 6989
反应条件
bis(dibenzylideneacetone)-palladium(0) in toluene T=23°C; Fukuyama reaction; Inert atmosphere;
参考文献
Kunchithapatham, Kamala; Eichman, Chad C.; Stambuli, James P.
Chemical Communications, 2011 , vol. 47, # 47 p. 12679 - 12681
反应条件
lt;2,2',3,3',5,5'-hexaphenyl-(1,1'-biphenyl)-4,4'-dioxylgt;; oxygen; copper(l) chloride in various solvent(s) T=95°C; 25.7333 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 35, # 32 p. 5833 - 5836
反应条件
tetrachlorosilane; silver perchlorate; [3H]-Caproic acid in dichloromethane 24 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 12 p. 3729 - 3734
反应条件
1: ethanol / 24 h / Heating 2: O2, CuCl, <2,2',3,3',5,5'-hexaphenyl-(1,1'-biphenyl)-4,4'-dioxyl> / various solvent(s) / 25.73 h / 95 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 32 p. 5833 - 5836
反应条件
potassium hydroxide in ethanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 44, p. 177 - 184
