N-(2-甲基-2-硝基丙基)苯胺合成路线 (共 5 条)
反应条件
N-benzyl-trimethylammonium hydroxide in methanol; water
7 h; Heating / reflux;
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP1354882 A1, 2003 ;
Location in patent: Page/Page column 85 ;
反应条件
tetrakis(2-hydroxyethyl)ammonium hydroxide
参考文献
Johnson
Journal of the American Chemical Society, 1946 , vol. 68, p. 14,16
反应条件
in ethanol
T=20°C; 24 h; other sodium alkylnitronates, N-(α-amidoalkyl)- and N-(α-aminoalkyl)- benzotriazoles; var. solvent, time, and temp.; Product distributionMechanism;
参考文献
Karitzky, Alan R.; Saczewski, Franciszek
Gazzetta Chimica Italiana, 1990 , vol. 120, # 6 p. 375 - 378
参考文献
Johnson
Journal of the American Chemical Society, 1946 , vol. 68, p. 14,16
反应条件
1: With hydrogenchloride; zinc in methanol; water
T=20°C; 2 h;
2: With ammonia in water
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP1354882 A1, 2003 ;
Location in patent: Page/Page column 85 ;