(2-氨基-2-甲基丙基)(丙烷-2-基)胺合成路线 (共 12 条)
参考文献
Journal of Organic Chemistry, , vol. 15, p. 68,70
反应条件
methanol; nickel
T=30 - 50°C; P=25742.8 Torr; Hydrogenation;
参考文献
Senkus
Journal of the American Chemical Society, 1946 , vol. 68, p. 11
Full Text Show Details
Comm.Solv.Corp.
Patent: US2393825 ;
反应条件
1: 92 percent / NaN3 / dimethylsulfoxide / 16 h / 50 °C
2: 86 percent / LiAlH4 / diethyl ether / 2 h / Heating
View Scheme
参考文献
De Kimpe; D'Hondt
Synthesis, 1993 , # 10 p. 1013 - 1017
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Asinger,F. et al.
Monatshefte fuer Chemie, 1967 , vol. 98, # 5 p. 1832 - 1842
反应条件
(i), (ii) (catalytic hydrogenation); Multistep reaction;
参考文献
De Kimpe,N. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3704 - 3708
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water
T=5°C; Yields of byproduct given;
参考文献
Lai, John T.
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 754 - 755
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=5°C;
参考文献
Lai, John T
Synthesis, 1981 , # 1 p. 40 - 42
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water
T=5°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai, John T.
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 754 - 755
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=5°C; Title compound not separated from byproducts;
参考文献
Lai, John T
Synthesis, 1981 , # 1 p. 40 - 42
参考文献
Riebsomer
Journal of the American Chemical Society, 1948 , vol. 70, p. 1629,1630, 1631