4-(4-甲氧基苯基)-2,6-二甲基-吡啶-3,5-二羧酸二乙酯合成路线 （共 7 条）
反应条件
in tetrachloromethane
3 h; Ambient temperatureIrradiation;
参考文献
Memarian, Hamid R.; Ghazaie, Marieh; Mehneh, Somayeh Kakhki
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2009 , vol. 64, # 10 p. 1187 - 1192
反应条件
ammonium chlorate
T=80°C; Hantzsch pyridine synthesis; 0.666667 h; Neat (no solvent);
参考文献
Nasr-Esfahani, Masoud; Karami, Bahador; Behzadi, Masoume
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 5 p. 931 - 935
反应条件
anhydrous potassium sulfate; potassium hydrogensulfate; oxone in acetonitrile
0.166667 h; Heating;
参考文献
Liu, Zhengang; Yu, Wei; Yang, Li; Liu, Zhong-Li
Tetrahedron Letters, 2007 , vol. 48, # 30 p. 5321 - 5324
反应条件
1: 23 percent / aq. NH4OH / 0.17 h / 140 °C / microwave irradiation
2: 99 percent / MnO2 / CH2Cl2 / 0.02 h / 100 °C / microwave irradiation
View Scheme
参考文献
Bagley, Mark C.; Lubinu, M. Caterina
Synthesis, 2006 , # 8 p. 1283 - 1288
反应条件
1: 23 percent / aq. NH4OH / 0.17 h / 140 °C / microwave irradiation
2: 99 percent / MnO2 / CH2Cl2 / 0.02 h / 100 °C / microwave irradiation
View Scheme
参考文献
Bagley, Mark C.; Lubinu, M. Caterina
Synthesis, 2006 , # 8 p. 1283 - 1288
反应条件
2: CrO3; acetic acid
View Scheme
参考文献
Borsche; Hahn
Justus Liebigs Annalen der Chemie, 1939 , vol. 537, p. 219,242
反应条件
in acetonitrile
T=24.84°C; Thermodynamic data;
参考文献
Zhu, Xiao-Qing; Liu, Qiao-Yun; Chen, Qiang; Mei, Lian-Rui
Journal of Organic Chemistry, 2010 , vol. 75, # 3 p. 789 - 808
