N-对甲苯磺酰咪唑-3,3-二丙酸合成路线 (共 6 条)
反应条件
hydrogenchloride in water 2 h; Heating;
参考文献
Pratt, John A. E.; Sutherland, Ian O.; Newton, Roger F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 13 - 22
反应条件
sodium hydroxide 1.) 1h, 2.) 1h, reflux;
参考文献
Beddoes, Roy L.; Edwards, W. D.; Joule, J. A.; Mills, O. S.; Street, J. D.
Tetrahedron, 1987 , vol. 43, # 8 p. 1903 - 1920
反应条件
1: 89 percent / pyridine / 10 deg C, 30 min, RT, 4 h 2: 95 percent / hydrochlorid acid / H2O / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 13 - 22
反应条件
1: 89 percent / pyridine / 10 deg C, 30 min, RT, 4 h 2: 95 percent / hydrochlorid acid / H2O / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 13 - 22
反应条件
1: BH3*S(CH3)2 2: pyridine / acetonitrile 3: KH / dimethylformamide 4: HBr 5: KOH / methanol View Scheme
参考文献
Erhardt,J.M.; Grover,E.R.; Wuest,J.D.
Journal of the American Chemical Society, 1980 , vol. 102, p. 6365
反应条件
1: BH3*S(CH3)2 2: pyridine / acetonitrile 3: KH / dimethylformamide 4: HBr View Scheme
参考文献
Erhardt,J.M.; Grover,E.R.; Wuest,J.D.
Journal of the American Chemical Society, 1980 , vol. 102, p. 6365