苯甲酰基-DL-alpha-丙氨酸乙酯合成路线 （共 17 条）
参考文献
Brenzinger
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1892 , vol. 16, p. 576
反应条件
hydrogen; Lindlar's catalyst in ethyl acetate
T=25°C; P=10343 Torr; 23 h;
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4902 - 4906
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4902 - 4906
反应条件
1: D2O / CHCl3
2: NaOEt / ethanol-d1 / 42 h / Ambient temperature
3: 26.3 g / CHCl3; H2O / 42 h
4: H2 / 5 percent Pd(CaCO3) / ethyl acetate / 23 h / 25 °C / 10343 Torr
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4902 - 4906
反应条件
1: 12.4 g / CHCl3; H2O / 42 h
2: H2 / 5 percent Pd/CaCO3 / ethyl acetate / 23 h / 25 °C / 10343 Torr
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4902 - 4906
反应条件
1: 26.3 g / CHCl3; H2O / 42 h
2: H2 / 5 percent Pd(CaCO3) / ethyl acetate / 23 h / 25 °C / 10343 Torr
View Scheme
参考文献
Aberhart, D. John; Russell, David J.
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4902 - 4906
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
insertion; Heating;
参考文献
Benati, Luisa; Nanni, Daniele; Sangiorgi, Corrado; Spagnolo, Piero
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7836 - 7841
反应条件
hydrogen in 1,4-dioxane
T=80°C; P=30003 Torr; 20 h; Autoclave;
参考文献
Hamasaki, Akiyuki; Liu, Xiaohao; Tokunaga, Makoto
Chemistry Letters, 2008 , vol. 37, # 12 p. 1292 - 1293
反应条件
triethylamine in dichloromethane
T=20°C; Aza-Wittig reaction; 4 h;
参考文献
Huang, Nian-Yu; Nie, Yi-Bo; Ding, Ming-Wu
Synlett, 2009 , # 4 p. 611 - 614
反应条件
triethylamine in acetonitrile
T=60°C; Aza-Wittig reaction;
参考文献
Huang, Nian-Yu; Nie, Yi-Bo; Ding, Ming-Wu
Synlett, 2009 , # 4 p. 611 - 614
