2-乙酰基苯基对茴香酸酯合成路线 （共 13 条）
反应条件
1: KOH / Heating 2: glacial acetic acid; H2SO4 / 100 °C View Scheme
参考文献
Nishinaga; Ando; Maruyama; Mashino
Synthesis, 1992 , # 9 p. 839 - 841
反应条件
sodium methylate in dimethyl sulfoxide T=30°C; substituent effects; acidity function correlations; Rate constant;
参考文献
Bowden, Keith; Chehel-Amiran, Mohsen
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 2039 - 2044
反应条件
1: 85 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 6 h / 20 °C 2: 77 percent / acetonitrile / 48 h / 20 °C 3: NaH / tetrahydrofuran / Heating 4: 357 mg / H2SO4 / acetic acid / 1.5 h / 60 °C 5: 88 percent / NaOH; H2O / ethanol / 2 h / 60 °C View Scheme
参考文献
Fougerousse, Andre; Gonzalez, Emmanuel; Brouillard, Raymond
Journal of Organic Chemistry, 2000 , vol. 65, # 2 p. 583 - 586
反应条件
1: 50 percent / ICl / acetic acid / 0.08 h / Heating 2: 50 percent / KOH / dioxane / 0.5 h / Heating View Scheme
参考文献
Joshi, M. G.; Wadokar, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 930 - 931
反应条件
sodium methylate in dimethyl sulfoxide T=30°C; substituent effects; acidity function correlations; Rate constant;
参考文献
Bowden, Keith; Chehel-Amiran, Mohsen
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 2039 - 2044
反应条件
tert.-butylhydroperoxide in water; dimethyl sulfoxide
T=80°C; 10 h; Inert atmosphere;
参考文献
Saberi, Dariush; Heydari, Akbar
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4178 - 4180
反应条件
tert.-butylhydroperoxide; copper diacetate in water; dimethyl sulfoxide
T=80°C; 20 h; Sealed tube;
参考文献
Sharma, Satyasheel; Park, Jihye; Kim, Mirim; Kwak, Jong Hwan; Jung, Young Hoon; Kim, In Su
Tetrahedron, 2013 , vol. 69, # 45 p. 9391 - 9397
反应条件
pyridine
T=20°C; Acylation; 2 h;
参考文献
Fougerousse, Andre; Gonzalez, Emmanuel; Brouillard, Raymond
Journal of Organic Chemistry, 2000 , vol. 65, # 2 p. 583 - 586
反应条件
pyridine; trichlorophosphate
T=50°C; 3 h;
参考文献
Naphade, V. J.; Ghiya, B. J.
Journal of the Indian Chemical Society, 1986 , vol. 63, p. 851 - 853
反应条件
1: AlCl3 / CS2
2: pyridine
View Scheme
参考文献
Bowden, Keith; Chehel-Amiran, Mohsen
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 2039 - 2044
