反应条件
1: 1.) NaH / 1.) 70 deg C, 45 min, 2.) THF, 25 deg C, 4 h 2: Ac2O / 0.75 h / 140 °C 3: aq. NaOH / methanol / 2 h / Heating 4: diethyl ether 5: phosphorous tribromide / 1.) 25 deg C, 12 h, 2.) 80 deg C, 1 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 10 p. 698 - 700
