1-甲基-1,4-二氮杂庚烷-5-酮合成路线 (共 4 条)
反应条件
sodium hydroxide; benzenesulfonyl chloride in acetone T=0 - 20°C; Beckmann rearrangement; 18 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 19 p. 2651 - 2653
反应条件
sodium azide; chloroform; sulfuric acid
参考文献
Journal of Organic Chemistry, , vol. 14, p. 530,534
Journal of Scientific and Industrial Research, , vol. 17 B, p. 31
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Sommers et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 5805
反应条件
1: LiAlH4; diethyl ether
2: Na2CO3; xylene
View Scheme
参考文献
Sommers et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 5805