2,4-二溴-6-乙炔基苯胺合成路线 （共 3 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 1 h;
参考文献
Koradin, Christopher; Dohle, Wolfgang; Rodriguez, Alain L.; Schmid, Bertram; Knochel, Paul
Tetrahedron, 2003 , vol. 59, # 9 p. 1571 - 1587
反应条件
1: 88 percent / I2; Ag2SO4 / ethanol / 3 h / 20 °C
2: 67 percent / CuI; Et3N; PdCl2(PPh3)2 / tetrahydrofuran / 3 h / 20 °C
3: 85 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
View Scheme
参考文献
Koradin, Christopher; Dohle, Wolfgang; Rodriguez, Alain L.; Schmid, Bertram; Knochel, Paul
Tetrahedron, 2003 , vol. 59, # 9 p. 1571 - 1587
反应条件
1: 67 percent / CuI; Et3N; PdCl2(PPh3)2 / tetrahydrofuran / 3 h / 20 °C
2: 85 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
View Scheme
参考文献
Koradin, Christopher; Dohle, Wolfgang; Rodriguez, Alain L.; Schmid, Bertram; Knochel, Paul
Tetrahedron, 2003 , vol. 59, # 9 p. 1571 - 1587
