N-苄基-4-甲基苯甲酰胺合成路线 （共 58 条）
反应条件
lanthanum trifluoromethanesulphonate
T=50°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Morimoto, Hiroyuki; Fujiwara, Risa; Shimizu, Yuhei; Morisaki, Kazuhiro; Ohshima, Takashi
Organic Letters, 2014 , vol. 16, # 7 p. 2018 - 2021
反应条件
[Ru(II)(η6-benzene)(μ-Cl)Cl]2; N,N-diisopropylimidazolium bromide; sodium hydride in toluene; acetonitrile
24 h; Inert atmosphereReflux;
参考文献
Chen, Cheng; Hong, Soon Hyeok
Organic Letters, 2012 , vol. 14, # 12 p. 2992 - 2995
反应条件
1: p-methylbenzaldehyde oxime With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene
T=130°C; 3 h; Inert atmosphereSchlenk techniqueGreen chemistry;
2: benzyl alcohol With caesium carbonate in toluene
T=130°C; 12 h; Inert atmosphereSchlenk techniqueGreen chemistry;
参考文献
Li, Feng; Qu, Panpan; Ma, Juan; Zou, Xiaoyuan; Sun, Chunlou
ChemCatChem, 2013 , vol. 5, # 8 p. 2178 - 2182
反应条件
N-Benzoyl-imidazole; potassium hydride in diethylene glycol dimethyl ether
T=90°C; 1 h;
参考文献
Bell, Christen M.; Kissounko, Denis A.; Gellman, Samuel H.; Stahl, Shannon S.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 5 p. 761 - 763
反应条件
N-Benzyldiacetamide; potassium hydride in diethylene glycol dimethyl ether
T=120°C; 18 h;
参考文献
Bell, Christen M.; Kissounko, Denis A.; Gellman, Samuel H.; Stahl, Shannon S.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 5 p. 761 - 763
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
oxygen; cobalt(II) chloride; sodium hydroxide in tetrahydrofuran; water
T=25°C; 12 h;
参考文献
Soule, Jean-Francois; Miyamura, Hiroyuki; Kobayashi, Shu
Journal of the American Chemical Society, 2011 , vol. 133, # 46 p. 18550 - 18553
反应条件
oxygen; copper(l) chloride in dimethyl sulfoxide
T=80°C; 0.5 h;
参考文献
Shibahara, Fumitoshi; Suenami, Aiko; Yoshida, Atsunori; Murai, Toshiaki
Chemical Communications, 2007 , # 23 p. 2354 - 2356
反应条件
potassium carbonate in toluene
T=120°C; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ghosh, Subhash C.; Chen, Anqi; Chai, Christina L. L.; Seayad, Abdul M.
Chemical Communications, 2012 , vol. 48, # 12 p. 1805 - 1807
