N-苄基-4-甲基苯甲酰胺合成路线 (共 58 条)
反应条件
sodium 2-methyl-2-adamantoxide; dichlorobis(dicyclohexylphosphinomethylpyridine)–ruthenium (II); hydrogen; sodium hydride in toluene; mineral oil T=160°C; P=45004.5 Torr; 24 h; Inert atmosphereAutoclave;
参考文献
Tetrahedron Letters, , vol. 54, # 21 p. 2674 - 2678
反应条件
sodium 2-methyl-2-adamantoxide; dichlorobis(dicyclohexylphosphinomethylpyridine)–ruthenium (II); hydrogen; sodium hydride in toluene; mineral oil T=160°C; P=45004.5 Torr; 24 h; Inert atmosphereAutoclave;
参考文献
Tetrahedron Letters, , vol. 54, # 21 p. 2674 - 2678
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=200°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 33 p. 11039 - 11050
反应条件
N-Benzoyl-imidazole; potassium hydride in diethylene glycol dimethyl ether T=90°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 5 p. 761 - 763
反应条件
N-Benzyldiacetamide; potassium hydride in diethylene glycol dimethyl ether T=120°C; 18 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 5 p. 761 - 763
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=200°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
反应条件
potassium superoxide; 18-crown-6 ether in benzene 168 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 37, p. 2313 - 2318
反应条件
trichloromonobromomethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine in tetrahydrofuran
T=60°C; 6 h; Inert atmosphere;
参考文献
Kawagoe, Yuhsuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2013 , vol. 69, # 19 p. 3971 - 3977
反应条件
1: 1-(iodo)-4-methylbenzene; benzylamine With sodium carbonate in water
0.166667 h; Autoclave;
2: carbon dioxide in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Revankar, Santosh A.; Khedkar, Mayur V.; Bhanage, Bhalchandra M.
Catalysis Today, 2012 , vol. 198, # 1 p. 148 - 153
反应条件
triethylamine in acetone
T=20°C; Cooling with ice;
参考文献
Al-Shawabkeh, Jumana D.; Al-Nadaf, Afaf H.; Dahabiyeh, Lina A.; Taha, Mutasem O.
Medicinal Chemistry Research, 2014 , vol. 23, # 1 p. 127 - 145