5-O-羰基甲氧基-1,2-o-异亚丙基-d-呋喃木糖合成路线 （共 14 条）
反应条件
1: With ammonium cerium (IV) nitrate in water; acetonitrile
T=20°C; 2 h;
2: With silica gel in ethanol; dichloromethane
Column chromatography;
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
aluminum oxide in ethanol; chloroform
Column chromatography;
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
ammonium cerium (IV) nitrate in water; acetonitrile
T=20°C; 2 h;
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
pyridine in chloroform
参考文献
Almond, Merrick R.; Collins, Jon L.; Reitter, Barbara E.; Rideout, Janet L.; Freeman, G. Andrew; St Clair, Marty H.
Tetrahedron Letters, 1991 , vol. 32, # 41 p. 5745 - 5748
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0 - 20 °C
2: pyridine; 4-(N,N-dimethlyamino)pyridine / 0 - 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C
View Scheme
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
1: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C
2: aluminum oxide / ethanol; chloroform / Column chromatography
View Scheme
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
1: pyridine; 4-(N,N-dimethlyamino)pyridine / 0 - 20 °C / Inert atmosphere
2: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C
3: aluminum oxide / ethanol; chloroform / Column chromatography
View Scheme
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0 - 20 °C
2: pyridine; 4-(N,N-dimethlyamino)pyridine / 0 - 20 °C / Inert atmosphere
3: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C
View Scheme
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0 - 20 °C
2.1: pyridine; 4-(N,N-dimethlyamino)pyridine / 0 - 20 °C / Inert atmosphere
3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C
3.2: Column chromatography
View Scheme
参考文献
Dvorakova, Marcela; Pribylova, Marie; Pohl, Radek; Migaud, Marie E.; Vanek, Tomas
Tetrahedron, 2012 , vol. 68, # 33 p. 6701 - 6711
