alpha-(乙酰基氨基)乙酰基乙酸乙酯合成路线 （共 34 条）
反应条件
Kochen des Reaktionsprodukts mit konz.wss.HCl;
参考文献
Albertson et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1150,1152
Full Text Show Details
Pfister et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 1101,1103
反应条件
Kochen des Reaktionsprodukts mit konz.wss.HCl;
参考文献
Albertson et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1150,1152
Full Text Show Details
Pfister et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 1101,1103
参考文献
Albertson et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1150,1152
反应条件
ethanol; sodium ethanolate Erhitzen des Reaktionsprodukts mit wss. HCl;
参考文献
Kawasaki
Nippon Kagaku Zasshi, 1957 , vol. 78, p. 1651
Chem.Abstr., 1960 , p. 1334
反应条件
thionyl chloride; benzene
参考文献
Ghosti, Arun K.; Kumaragurubaran, Nagaswamy; Hong, Lin; Lei, Hui; Hussain, Khaja Azhar; Liu, Chun-Feng; Devasamudram, Thippeswamy; Weerasena, Vajira; Turner, Robert; Koelsch, Gerald; Bilcer, Geoffrey; Tang, Jordan
Journal of the American Chemical Society, 2006 , vol. 128, # 16 p. 5310 - 5311
参考文献
Albertson et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1150,1152
参考文献
Albertson et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1150,1152
反应条件
hydrogen; palladium on activated charcoal
4 h; Ambient temperature;
参考文献
Soukup, Milan; Wipf, Beat; Hochuli, Erich; Leuenberger, Hans G. W.
Helvetica Chimica Acta, 1987 , vol. 70, p. 232 - 236
反应条件
1: ethyl acetoacetate With acetic acid; sodium nitrite in water
T=20°C; 3 h;
2: acetic anhydride With hydrogen; palladium 10 on activated carbon in acetic acid
P=2585.81 Torr; 1.5 h;
参考文献
ZAPAQ, INC.; THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS; OKLAHOMA MEDICAL RESEARCH FOUNDATION
Patent: WO2006/34277 A1, 2006 ;
Location in patent: Page/Page column 61-62 ;
WO 2006/034277 A1
反应条件
1: ethyl acetoacetate With acetic acid; sodium nitrite in water
T=20°C; 1 h;
2: acetic anhydride; acetic acid With hydrogen; palladium on activated carbon
P=2585.81 Torr; 1.5 h;
参考文献
Ghosh, Arun K.; Lei, Hui; Devasamudram, Thippeswamy; Tang, Jordan J. N.; Bilcer, Geoffrey; Liu, Chungfeng
Patent: US2008/125467 A1, 2008 ;
Location in patent: Page/Page column 20 ;
