5-苯基偶氮嘧啶-4,6-二胺合成路线 （共 6 条）
反应条件
ethanol; nickel T=100°C; P=36775.4 - 44130.5 Torr; Hydrogenation;
参考文献
Cavalieri; Tinker; Bendich
Journal of the American Chemical Society, 1949 , vol. 71, p. 535
反应条件
sodium ethanolate in ethanol
1.5 h, reflux, then RT.;
参考文献
Narita; Kitagawa; Hirai
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4928 - 4934
参考文献
Richter; Taylor
Journal of the American Chemical Society, 1956 , vol. 78, p. 5848,5850
参考文献
Richter; Taylor
Journal of the American Chemical Society, 1956 , vol. 78, p. 5848,5850
反应条件
1: 38 percent / dimethylformamide / 2 h / Ambient temperature
2: 89 percent / (CH3)2NH-MeOH / 12 h / Ambient temperature
View Scheme
参考文献
Mano; Seo; Imai
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3454 - 3459
反应条件
1: 38 percent / dimethylformamide / 2 h / Ambient temperature
2: 89 percent / (CH3)2NH-MeOH / 12 h / Ambient temperature
3: 52 percent / dimethylformamide / 2 h / Ambient temperature
4: 94 percent / 50percent (CH3)2NH/MeOH / 24 h / Ambient temperature
View Scheme
参考文献
Mano; Seo; Imai
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3454 - 3459
