1,10-菲罗啉-5-氨基合成路线 （共 9 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=2280.15 Torr; 1 h;
参考文献
Chemical Communications, , # 43 p. 4539 - 4541
反应条件
1: 63 percent / conc. HNO3, 18percent oleum / 2 h / 100 - 110 °C 2: 58 percent / SnCl2, hydrochloric acid / 1 h / 80 - 90 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, # 12 p. 2476 - 2479
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2701 - 2705
反应条件
hydrogenchloride; tin(ll) chloride T=120°C; 2 h;
参考文献
Chemistry - An Asian Journal, , vol. 8, # 11 p. 2822 - 2827
反应条件
in hydrogenchloride; acetic acid
反应条件
triethylamine in acetonitrile T=20°C; 24 h; Inert atmosphere;
参考文献
Xu, Cun-Jin; Li, Bo-Geng; Wan, Jin-Tao; Bu, Zhi-Yang
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 82, # 1 p. 159 - 163
反应条件
toluene-4-sulfonic acid in chloroform Heating;
参考文献
Ramiro, Pedro; Garcia-Fresnadillo, David; Orellana, Guillermo
Tetrahedron, 2005 , vol. 61, # 40 p. 9478 - 9483
反应条件
sodium acetate in N,N-dimethyl acetamide; water; acetone
0.0833333 h;
参考文献
Khimich; Obrezkov; Koptelova
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 4 p. 555 - 557
反应条件
1: cis-[Ru(2,2'-bipyridine)2Cl2]*2H2O; 5-Amino-1,10-phenanthroline in methanol
12 h; Inert atmosphereReflux;
2: NH4PF6 in methanol; water
0.166667 h; Inert atmosphere;
参考文献
Lou, Kun; Lovell, Jonathan F.
Chemical Communications, 2014 , vol. 50, # 24 p. 3231 - 3233
